Download PDF Handbook of Instrumental Techniques for Analytical Chemistry
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Handbook of Instrumental Techniques for Analytical Chemistry
Download PDF Handbook of Instrumental Techniques for Analytical Chemistry
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From the Publisher
This book/disk Handbook provides introductory information about the most widely used instrumental techniques and methods used in analytical chemistry and helps the reader determine which technique is most appropriate for their needs. This book/disk Handbook consists of an introduction and seven sections, each addressing a major area of chemical analysis (separation techniques, optical spectroscopic techniques-qualitative, optical spectroscopic techniques-quantitative, mass spectrometry, electrochemical techniques, microscopic and surface techniques, polymer and macromolecular techniques) and a floppy disk containing Technique Selection software. Each section consists of chapters describing the most commonly used instrumental techniques in the area of analysis. Each chapter presents basic information about a specific technique. The common format used for each chapter facilitates selection and comparison of techniques. Each chapter contains the following topics: 1) a summary page, 2) how it works, 3) what it does including current applications, 4) types of samples analyzed, practical economic information, 5) summary of the routine operational characteristics, and 6) references to more detailed information on the technique.
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From the Back Cover
Chemical Analysis is not just for analytical chemists! Scientists, engineers, and technicians in a variety of fields often need information from chemical analyses in their work. Many professional chemists also require information from techniques outside their area of specialization. With this handbook, these users can find information about the most common analytical chemical techniques in an understandable form, simplifying decisions about which analytical techniques can provide the information they are seeking on chemical composition and structure. Compiled by experts in each specialty, the handbook uses a standardized format to facilitate the comparison of techniques. Each chapter features: * A quick-look summary * How the technique works * What information the technique can provide and how it's used * Economic considerations * Routine operational characteristics * Reference sources for more detailed study * A comprehensive glossary defines technical terms and acronyms. The handbook covers widely used techniques in the areas: * Electromagnetic spectrometry * Separation techniques * Mass spectrometry * Electrochemistry * Microscopy and surface techniques * Polymers and macromolecules A general introductory section addresses issues associated with: * The process of obtaining chemical information from samples * Preparation of organic and inorganic samples * Accessing the quality of measurements * Laboratory automation * Laboratory information systems Persons in areas such as biotechnology, materials science, environmental science, and geology will find the Handbook provides an understandable overview and useful introduction to techniques that can provide information to solve problems. The Handbook's wide range and standardized format make it the ideal reference work for anyone who uses chemical analyses in their work. The enclosed Technique Selection Program can be used in two ways. In the first mode, users follow a series of menus to describe both the characteristics of their samples and the information they desire from the sample. They then receive a reference to appropriate analysis techniques described in the text. In the second mode, they can select from a listing of the techniques discussed in the book to obtain quick information about each method's applicability, including the characteristics of samples it can analyze, and the types of information the analysis provides.
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Product details
Hardcover: 995 pages
Publisher: Prentice Hall (June 4, 1997)
Language: English
ISBN-10: 0131773380
ISBN-13: 978-0131773387
Product Dimensions:
8.2 x 1.8 x 10.2 inches
Shipping Weight: 4.6 pounds
Average Customer Review:
2.4 out of 5 stars
4 customer reviews
Amazon Best Sellers Rank:
#1,521,389 in Books (See Top 100 in Books)
The content of the book is great and I have no complaints. The coverage of instrumental analysis techniques is quite complete, although some procedures such as Mossbauer spectroscopy and instrumental neutron activation analysis are not discussed. My problem is that I paid for a new book and was sent an inferior "Low Cost Edition" that was printed in India and expressly for sale only in Asia - I live in the U.S. The book was also used and had the previous owner's name whited out in the inside front cover. An illegal, low cost used book is not what I ordered.
I bought the 1997 edition of this book, with CD, in 2001 for $70.00 -- I cannot recommend it as being worth more than that. I really didn't find it to be very useful for my original intent, which was to have a good reference for instrumental techniques, including those used in pharmaceutical and biological research. The CD included with the book has a simple, almost DOS level, program that installs and aids to some small extent in picking specific methods to do analysis of some sample type you input. My only comment is that, if you need this kind of gimmick to choose your analytical method, you would be better off getting into a job or a class that uses current analytical instrumentation.Having seen the current offering price and since I still have the book, little used, my quandary is whether I should be offering it for some highly inflated price, or go ahead and give it to the Goodwill as I was about to do.
Have you ever tried to explain what analytical chemistry is, to a friend, relative, or stranger feigning interest in what you do? The attempt quickly reveals the depth and complexity of a field so easily named with two simple words. Where do you begin? What do you leave out? Trying to write a textbook on the many facets of analytical chemistry is even more difficult; some attempts run to many volumes. Some texts focus on the physical principles of a technique, others on the applications. Prentice-Hall's new Handbook of Instrumental Techniques for Analytical Chemistry (Frank Every lab occasionally faces a problem outside the usual routine - questions their normal instruments can't answer. The Handbook helps them figure out what instruments might do the job. The goal of the book is to introduce nonspecialist scientists to the major techniques, outlining how each works, what it does, its limitations, the information produced, plus practical matters such as costs to buy and operate, and the expertise required of an operator. Each chapter has a list of manufacturers and a bibliography for further self-education. A person who goes through a chapter will be ready to ask intelligent questions of experts in the field and understand the buzzwords peculiar to each discipline. The book contains a CD-ROM with software for selecting appropriate methods for a sample and analysis; since it runs on Windows (3.1, 95, or NT), I couldn't test it on my Macintosh. The authors of the chapters are a mix of university researchers, innovators from industry, and a few carefully-selected experts from instrument companies, who avoid the temptation to promote their own products. For example, the STM/AFM chapter was written by Huub Salemink of the IBM labs in Zurich, where the technique was pioneered. Although I don't want to slight any of the excellent authors who contributed chapters, some areas are truly outstanding texts in their own right. Ron Majors' discussion of organic sample preparation is as thorough as readers of his LC*GC columns would expect. Robert Megargle covers LIMS with the knowledge of many years as user and observer. Defining categories for the overlapping techniques of analytical chemistry is always a challenge. Settle wisely avoided the traditional choice of categorization by underlying physical principles and grouped them according to logical applications. The result includes some based on the instrument types (separation methods, for example) and others on broad application areas (polymer analysis). While purists might fret over this organization, in fact, it makes for easy access, without having to shuffle through the whole book to gather information on a specific analysis. In a single volume covering fields that are often evolving rapidly, there are bound to be a few omissions. The ones I noted were: near infrared (NIR) spectroscopy, which has become so important recently; microscopy other than SPM, especially the analytical use of electron microscopes (SEM and TEM); better discussions of time-of-flight and ion trap mass spec; ion sources other than ESI for LC-MS; microwave ovens used for digestion and extraction of inorganic samples (Majors covers its use in organic extraction); flow injection (and segmented-flow) analysis; arc-spark emission spectrometers (mentioned in passing). To really pick nits, there was no mention of solid phase microextraction (SPME) or of specialized analyzers such as CHN, TOC, BOD, or systems for Hg, CN, or S analysis. At the same time, it includes a chapter on the truly exotic and rare technique of atomic fluorescence. Any manageable text will overlook some methods and cover some obscure favorites; this criticism is hardly fatal. Any book on an evolving technology is a snapshot in time and will fairly quickly become dated. The newest techniques have already gone beyond the descriptions in their chapters. This text, nevertheless, will be an excellent introduction to analytical instrument techniques for some years, even if the published prices and suppliers' names may age. I hope some of the more enlightened professors of instrumental analysis will use it as a text; their students will emerge as better analytical chemists. It will certainly help me better understand the techniques I survey each month. Excerpted with permission from Analytical Consumer, Jo Rita Jordan, Editor and Publisher
This book is a must for the instrumental chemist. It covers it some detail most general and specialized instrumental techniques employed by chemist. It also gives specific applications of these techniques, manufacturers of instruments and supplies, and estimates on costs. In my lab I often find people first refering to this book when reviewing a new technique or wishing to 'brush up' on a technique they have not used in a while. It is a good first reference and I reccomend it to any analytical chemist.
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